Controlled synthesis of labelled 3-L-chlorotyrosine-[ring-C-13(6)] and of 3,5-L-dichlorotyrosine-[ring-C-13(6)]
Articolo
Data di Pubblicazione:
2004
Citazione:
Controlled synthesis of labelled 3-L-chlorotyrosine-[ring-C-13(6)] and of 3,5-L-dichlorotyrosine-[ring-C-13(6)] / P. Allevi, P. Olivero, M. Anastasia. - In: JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS. - ISSN 0362-4803. - 47:13(2004 Nov), pp. 935-945.
Abstract:
Pure 3-L-chlorotyrosine-[ring-C-13(6)] is prepared by chlorination of the 5-oxazolidinone of L-tyrosine-[ring-C-13(6)] with SO2Cl2 in CH3COOH-Et2O and successive one-pot regeneration of the protected aminoacidic functions by BCl3 in dichloromethane
Tipologia IRIS:
01 - Articolo su periodico
Keywords:
Sodium-hydrogen carbonate ; amino-acids ; sulfuryl chloride ; hypochlorous acid ; tyrosyl residues ; alkyl esters ; myeloperoxidase ; chlorination ; 3-chlorotyrosine ; neutrophils
Elenco autori:
P. Allevi, P. Olivero, M. Anastasia
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