Gas- chromatographic determination of pig plasma malondialdehyde with negative-ion chemical ionization tandem mass spectrometry detection
Articolo
Data di Pubblicazione:
1999
Citazione:
Gas- chromatographic determination of pig plasma malondialdehyde with negative-ion chemical ionization tandem mass spectrometry detection / L.M. Chiesa, K. De Wasch, A.M. Pecile, P.A. Biondi, H. De Brabander. - In: ARCHIV FÜR LEBENSMITTELHYGIENE. - ISSN 0003-925X. - 50:2(1999), pp. 41-43.
Abstract:
Malondialdehyde (MDA) was estimated in pig plasma by gas chromatography with NICI-MS-MS detection after derivatization with pentafluorobenzyl hydroxylamine. Glutaraldehyde was used as an internal standard. MDA gave two peaks, only the major one was considered for quantitative analysis. In multiple reaction monitoring mode the minimum detectable amount was 40 pmoles per sample. In 9 pig plasma samples, collected at abattoir, the MDA contents found were between 220-1015 pmoles/ml.
Tipologia IRIS:
01 - Articolo su periodico
Elenco autori:
L.M. Chiesa, K. De Wasch, A.M. Pecile, P.A. Biondi, H. De Brabander
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