Data di Pubblicazione:
1997
Citazione:
The contribution of powder diffraction methods to structural co-ordination chemistry / N. Masciocchi, A. Sironi. - In: JOURNAL OF THE CHEMICAL SOCIETY DALTON TRANSACTIONS. - ISSN 0300-9246. - :24(1997), pp. 4643-4643-+.
Abstract:
Ab-initio X-ray powder diffraction (see cover for typical spectra) is shown to be a powerful structural tool for (i) insoluble, thermally unstable, compounds which cannot be (re)crystallised from solution or from the melt; (ii) metastable phases destroyed or modified upon manipulation; (iii) twins; (iv) very small crystals and/or crystal aggregates; (v) gas/solid, liquid/solid and solid-state reactions fragmenting and misorienting the coherent domains of the starting crystals but conserving the (poly)crystalline nature of the sample.
Tipologia IRIS:
01 - Articolo su periodico
Keywords:
CRYSTAL-STRUCTURE DETERMINATION ; X-RAY-DIFFRACTION ; INITIO STRUCTURE ; DETERMINATION ; SYNCHROTRON-RADIATION ;
NEUTRON-DIFFRACTION ; POLYMER ; ELECTROLYTES ; COMPLEX STRUCTURES ;
PHASES ; FORM ; DIFFRACTOMETRY
Elenco autori:
N. Masciocchi, A. Sironi
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