Validation Study of Analysis of 1-Phenyl-2-Propanone in Illicit Methamphetamine Samples by Dynamic Headspace Gas Chromatography Mass Spectrometry
Articolo
Data di Pubblicazione:
2016
Citazione:
Validation Study of Analysis of 1-Phenyl-2-Propanone in Illicit Methamphetamine Samples by Dynamic Headspace Gas Chromatography Mass Spectrometry / S. Arnoldi, G. Roda, E. Casagni, A. Coceanig, L. Dell’Acqua, F. Farè, C. Rusconi, L. Tamborini, G.L. Visconti, V. Gambaro. - In: JOURNAL OF CHROMATOGRAPHY & SEPARATION TECHNIQUES. - ISSN 2157-7064. - 7:2(2016). [10.4172/2157-7064.1000322]
Abstract:
A new method based on dynamic headspace sampling (DHS) coupled to GC/MS analysis was developed, optimized and validated for the analysis of 1-phenyl-2-propanone (P2P) in illicit methamphetamine (MAMP) samples. The DHS parameters were investigated to reach the sensitivity suitable for this kind of analysis. The method showed of a good specificity, linearity, accuracy, precision and robustness. The analysis of ten MAMP samples seized by the judicial authority was carried out. P2P was found in all the seizure, confirming that P2P is the starting compound of the synthesis of amphetamines.
Tipologia IRIS:
01 - Articolo su periodico
Keywords:
1-phenyl-2-propanone; P2P; methamphetamine; DHSGC/MS
Elenco autori:
S. Arnoldi, G. Roda, E. Casagni, A. Coceanig, L. Dell’Acqua, F. Farè, C. Rusconi, L. Tamborini, G.L. Visconti, V. Gambaro
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